Information card for entry 7006019

Structure parameters

• Formula: C18 H50 B N3 Na P Si2
• Calculated formula: C18 H50 B N3 Na P Si2
• SMILES: [Na]123([N](C)(C)CC[N]1(C)CC[N]2(C)C)[H][BH2][P](C3([Si](C)(C)C)[Si](C)(C)C)(C)C
• Title of publication: Alkali metal complexes of a phosphine-borane-stabilised carbanion: influence of co-ligands on structure.
• Authors of publication: Izod, Keith; Wills, Corinne; Clegg, William; Harrington, Ross W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 33
• Pages of publication: 3669 - 3675
• a: 9.1995 ± 0.001 Å
• b: 15.3391 ± 0.0017 Å
• c: 20.149 ± 0.002 Å
• α: 90°
• β: 99.899 ± 0.002°
• γ: 90°
• Cell volume: 2800.9 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0621
• Residual factor for significantly intense reflections: 0.0423
• Weighted residual factors for significantly intense reflections: 0.0968
• Weighted residual factors for all reflections included in the refinement: 0.1072
• Goodness-of-fit parameter for all reflections included in the refinement: 1.068
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No