Information card for entry 7006097

Structure parameters

• Formula: C22 H24.5 Cl4 N4.5 Ni O5.5 Re
• Calculated formula: C22 H21.5 Cl4 N4.5 Ni O5.5 Re
• Title of publication: Synthesis, crystal structure and magnetic properties of novel heterobimetallic malonate-bridged MIIReIV complexes (M = Mn, Fe, Co and Ni)
• Authors of publication: Cuevas, Alicia; Kremer, Carlos; Suescun, Leopoldo; Russi, Silvia; Mombrú, Alvaro W.; Lloret, Francesc; Julve, Miguel; Faus, Juan
• Journal of publication: Dalton Transactions
• Year of publication: 2007
• Journal issue: 45
• Pages of publication: 5305
• a: 8.0455 ± 0.0003 Å
• b: 13.365 ± 0.007 Å
• c: 14.493 ± 0.008 Å
• α: 73.86 ± 0.04°
• β: 85.12 ± 0.04°
• γ: 77.55 ± 0.04°
• Cell volume: 1461.3 ± 1.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.2427
• Residual factor for significantly intense reflections: 0.097
• Weighted residual factors for significantly intense reflections: 0.2291
• Weighted residual factors for all reflections included in the refinement: 0.3007
• Goodness-of-fit parameter for all reflections included in the refinement: 0.961
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No