Information card for entry 7006111

Structure parameters

• Formula: C15 H27 Cl2 N2 P Pd
• Calculated formula: C15 H27 Cl2 N2 P Pd
• SMILES: [Pd]1(Cl)(Cl)[P](CN(c2[n]1cccc2)C)(C(C)(C)C)C(C)(C)C
• Title of publication: Steric control over the formation of cis and trans bis-chelated palladium(II) complexes using a new series of flexible N,P pyridyl-phosphine ligands.
• Authors of publication: Clarke, Deborah A.; Miller, Philip W.; Long, Nicholas J.; White, Andrew J. P.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 40
• Pages of publication: 4556 - 4564
• a: 8.5961 ± 0.0013 Å
• b: 13.265 ± 0.002 Å
• c: 16.3961 ± 0.0003 Å
• α: 90°
• β: 105.141 ± 0.005°
• γ: 90°
• Cell volume: 1804.7 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0228
• Residual factor for significantly intense reflections: 0.0205
• Weighted residual factors for significantly intense reflections: 0.0505
• Weighted residual factors for all reflections included in the refinement: 0.0515
• Goodness-of-fit parameter for all reflections included in the refinement: 1.107
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No