Information card for entry 7006183

Structure parameters

• Formula: C4.5 H10 Ga3 N O14 P3
• Calculated formula: C4.5 Ga3 N O14 P3
• Title of publication: Ionothermal synthesis, crystal structure and solid-state NMR spectroscopy of a new organically templated gallium oxalatophosphate: (H2TMPD)0.5[Ga3(C2O4)0.5(PO4)3] (TMPD=N,N,N',N'-tetramethyl-1,3-propanediamine).
• Authors of publication: Tang, Ming-Feng; Liu, Yi-Hui; Chang, Pai-Ching; Liao, Yi-Chen; Kao, Hsien-Ming; Lii, Kwang-Hwa
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 40
• Pages of publication: 4523 - 4528
• a: 8.9999 ± 0.0008 Å
• b: 9.1123 ± 0.0008 Å
• c: 9.4932 ± 0.0008 Å
• α: 90.837 ± 0.001°
• β: 94.231 ± 0.001°
• γ: 94.178 ± 0.001°
• Cell volume: 774.19 ± 0.12 ų
• Cell temperature: 294 ± 2 K
• Ambient diffraction temperature: 294 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0362
• Residual factor for significantly intense reflections: 0.031
• Weighted residual factors for significantly intense reflections: 0.0752
• Weighted residual factors for all reflections included in the refinement: 0.0774
• Goodness-of-fit parameter for all reflections included in the refinement: 1.073
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No