Information card for entry 7006225

Structure parameters

• Common name: Bis(tetrahydrofurane)-thiobis(6-tert-butyl-4-methylphenolato)- triphenylmethoxy-lutetium(iii)
• Chemical name: Bis(tetrahydrofurane)-thiobis(6-tert-butyl-4-methylphenolato)- triphenylmethoxy-lutetium(III)
• Formula: C55.75 H74 Lu O5.75 S
• Calculated formula: C55.75 H74 Lu O5.75 S
• Title of publication: Lutetium alkyl and hydride complexes in a non-cyclopentadienyl coordination environment.
• Authors of publication: Konkol, Marcin; Spaniol, Thomas P.; Kondracka, Małgorzata; Okuda, Jun
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 36
• Pages of publication: 4095 - 4102
• a: 33.017 ± 0.005 Å
• b: 18.291 ± 0.003 Å
• c: 20.635 ± 0.003 Å
• α: 90°
• β: 108.832 ± 0.003°
• γ: 90°
• Cell volume: 11795 ± 3 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0936
• Residual factor for significantly intense reflections: 0.0501
• Weighted residual factors for significantly intense reflections: 0.1294
• Weighted residual factors for all reflections included in the refinement: 0.1488
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No