Information card for entry 7006227

Structure parameters

• Common name: Bis(tetrahydrofurane)-mu-hydrido-thiobis(6-tert-butyl-4- methylphenolato)-lutetium(iii) dimer
• Chemical name: Bis(tetrahydrofurane)-μ-hydrido-thiobis(6-tert-butyl-4-methylphenolato)- lutetium(III) dimer
• Formula: C39 H65 Lu O5 S
• Calculated formula: C39 H65 Lu O5 S
• Title of publication: Lutetium alkyl and hydride complexes in a non-cyclopentadienyl coordination environment.
• Authors of publication: Konkol, Marcin; Spaniol, Thomas P.; Kondracka, Małgorzata; Okuda, Jun
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 36
• Pages of publication: 4095 - 4102
• a: 29.835 ± 0.009 Å
• b: 17.805 ± 0.006 Å
• c: 18.098 ± 0.006 Å
• α: 90°
• β: 121.466 ± 0.005°
• γ: 90°
• Cell volume: 8200 ± 5 ų
• Cell temperature: 140 ± 2 K
• Ambient diffraction temperature: 140 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0332
• Residual factor for significantly intense reflections: 0.0256
• Weighted residual factors for significantly intense reflections: 0.0633
• Weighted residual factors for all reflections included in the refinement: 0.0682
• Goodness-of-fit parameter for all reflections included in the refinement: 0.987
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No