Information card for entry 7006235

Structure parameters

• Formula: C358 H308 La12 O64
• Calculated formula: C352 H276 La12 O64
• Title of publication: Templated assembly of a mu6-CO3 2- dodecanuclear lanthanum dibenzoylmethanide hydroxido cluster with concomitant formation of phenylglyoxylate.
• Authors of publication: Andrews, Philip C.; Beck, Tobias; Forsyth, Craig M.; Fraser, Benjamin H.; Junk, Peter C.; Massi, Massimiliano; Roesky, Peter W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 48
• Pages of publication: 5651 - 5654
• a: 19.861 ± 0.004 Å
• b: 21.886 ± 0.004 Å
• c: 22 ± 0.004 Å
• α: 107.81 ± 0.03°
• β: 111.54 ± 0.03°
• γ: 102.31 ± 0.03°
• Cell volume: 7876 ± 5 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0681
• Residual factor for significantly intense reflections: 0.0536
• Weighted residual factors for significantly intense reflections: 0.1135
• Weighted residual factors for all reflections included in the refinement: 0.1229
• Goodness-of-fit parameter for all reflections included in the refinement: 1.098
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No