Information card for entry 7006250

Structure parameters

• Formula: C61 H57 Br N4 O3 P4 W
• Calculated formula: C61 H53 Br N4 O3 P4 W
• Title of publication: The oxadiazolyldiazenido(1-) ligand: a remarkably versatile platform for the synthesis of heteropolynuclear transition metal complexes.
• Authors of publication: Colquhoun, Howard M.; Chan, Yun Fu; Cardin, Christine J.; Drew, Michael G. B.; Gan, Yu; Abd El Kader, Kareem; White, Terence M.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 35
• Pages of publication: 3864 - 3867
• a: 16.69 ± 0.009 Å
• b: 17.33 ± 0.003 Å
• c: 20.19 ± 0.005 Å
• α: 90°
• β: 90.54 ± 0.04°
• γ: 90°
• Cell volume: 5839 ± 4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1218
• Residual factor for significantly intense reflections: 0.0841
• Weighted residual factors for significantly intense reflections: 0.1804
• Weighted residual factors for all reflections included in the refinement: 0.1893
• Goodness-of-fit parameter for all reflections included in the refinement: 0.841
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: Cukα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No