Information card for entry 7006443

Structure parameters

• Formula: C22 H58 K2 O2 Si6
• Calculated formula: C22 H58 K2 O2 Si6
• Title of publication: Alkali metal complexes of sterically hindered mono- and di-carbanions containing Si-O bonds.
• Authors of publication: Bowman, Lyndsey J.; Izod, Keith; Clegg, William; Harrington, Ross W.; Smith, J. David; Eaborn, C.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 3
• Pages of publication: 502 - 508
• a: 15.3506 ± 0.0007 Å
• b: 11.8073 ± 0.0005 Å
• c: 20.1478 ± 0.0009 Å
• α: 90°
• β: 98.5763 ± 0.0007°
• γ: 90°
• Cell volume: 3610.9 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0623
• Residual factor for significantly intense reflections: 0.0454
• Weighted residual factors for significantly intense reflections: 0.1212
• Weighted residual factors for all reflections included in the refinement: 0.1368
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No