Information card for entry 7006569

Structure parameters

• Formula: C21 H34 Co O3 P Si
• Calculated formula: C21 H34 Co O3 P Si
• Title of publication: The synthesis, characterisation and reactivity of 2-phosphanylethylcyclopentadienyl complexes of cobalt, rhodium and iridium.
• Authors of publication: McConnell, Ann C.; Pogorzelec, Peter J.; Slawin, Alexandra M. Z.; Williams, Gary L.; Elliott, Paul I. P.; Haynes, Anthony; Marr, Andrew C.; Cole-Hamilton, David J
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 1
• Pages of publication: 91 - 107
• a: 8.7 ± 0.003 Å
• b: 10.216 ± 0.003 Å
• c: 14.368 ± 0.005 Å
• α: 92.9 ± 0.007°
• β: 96.994 ± 0.006°
• γ: 100.669 ± 0.006°
• Cell volume: 1242.1 ± 0.7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.2326
• Residual factor for significantly intense reflections: 0.089
• Weighted residual factors for all reflections: 0.3622
• Weighted residual factors for significantly intense reflections: 0.2104
• Goodness-of-fit parameter for all reflections: 0.705
• Goodness-of-fit parameter for significantly intense reflections: 0.874
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No