Information card for entry 7006619

Structure parameters

• Formula: C36 H81 Lu O12 Si3
• Calculated formula: C36 H81 Lu O12 Si3
• Title of publication: Synthesis, structure and hydrosilylation activity of neutral and cationic rare-earth metal silanolate complexes.
• Authors of publication: Elvidge, Benjamin R.; Arndt, Stefan; Spaniol, Thomas P.; Okuda, Jun
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 7
• Pages of publication: 890 - 901
• a: 11.9494 ± 0.0007 Å
• b: 13.9573 ± 0.0009 Å
• c: 14.4939 ± 0.0009 Å
• α: 86.712 ± 0.001°
• β: 76.002 ± 0.001°
• γ: 88.549 ± 0.001°
• Cell volume: 2341.5 ± 0.3 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0459
• Residual factor for significantly intense reflections: 0.0392
• Weighted residual factors for significantly intense reflections: 0.0967
• Weighted residual factors for all reflections included in the refinement: 0.1109
• Goodness-of-fit parameter for all reflections included in the refinement: 1.128
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No