Information card for entry 7006715

Structure parameters

• Common name: Mn-complex perchlorate
• Chemical name: Mn-complex perchlorate
• Formula: C24 H36 Cl2 Mn N10 O8
• Calculated formula: C24 H36 Cl2 Mn N10 O8
• Title of publication: Synthesis and characterization of manganese(II) and iron(III) d5 tripodal imidazole complexes. Effect of oxidation state, protonation state and ligand conformation on coordination number and spin state.
• Authors of publication: Brewer, Cynthia; Brewer, Greg; Butcher, Ray J.; Carpenter, Everett E.; Cuenca, Luciann; Noll, Bruce C.; Scheidt, W. Robert; Viragh, Carol; Zavalij, Peter Y.; Zielaski, Daniel
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 8
• Pages of publication: 1009 - 1019
• a: 11.8154 ± 0.0005 Å
• b: 12.2056 ± 0.0006 Å
• c: 12.3982 ± 0.0006 Å
• α: 78.863 ± 0.001°
• β: 70.789 ± 0.001°
• γ: 67.4 ± 0.001°
• Cell volume: 1554.2 ± 0.13 ų
• Cell temperature: 233 ± 2 K
• Ambient diffraction temperature: 233 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0411
• Residual factor for significantly intense reflections: 0.0369
• Weighted residual factors for significantly intense reflections: 0.0809
• Weighted residual factors for all reflections included in the refinement: 0.0836
• Goodness-of-fit parameter for all reflections included in the refinement: 1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No