Information card for entry 7006734

Structure parameters

• Common name: (Salen)Sc(OSitBuPh2)
• Chemical name: [N,N'-bis(3,5-di-tert.-butylsalicylidene)ethylene diamino](diphenyl-tert. -butylsiloxy)scandium(III) (Salen)Sc(OSitBuPh2)
• Formula: C48 H65 N2 O3 Sc Si
• Calculated formula: C48 H65 N2 O3 Sc Si
• Title of publication: Synthesis and structural characterization of scandium SALEN complexes.
• Authors of publication: Meermann, Christian; Sirsch, Peter; Törnroos, Karl W; Anwander, Reiner
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 8
• Pages of publication: 1041 - 1050
• a: 12.056 ± 0.0002 Å
• b: 14.0187 ± 0.0002 Å
• c: 16.0392 ± 0.0003 Å
• α: 66.9842 ± 0.0006°
• β: 75.4467 ± 0.0006°
• γ: 67.8923 ± 0.0006°
• Cell volume: 2294.25 ± 0.07 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1111
• Residual factor for significantly intense reflections: 0.0594
• Weighted residual factors for significantly intense reflections: 0.1031
• Weighted residual factors for all reflections included in the refinement: 0.1176
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No