Information card for entry 7006785

Structure parameters

• Formula: C34 H50 Ag2 F6 N6 O8 S8
• Calculated formula: C35.66 H50 Ag2 F5.64 N6 O6.36 S7.38
• Title of publication: Dimetallo[3.3]para- and metacyclophanes by self-assembly of pyridylmethyl armed-monoazatrithia- and monoazadithiaoxa-12-crown-4 ethers with Ag+ ions.
• Authors of publication: Habata, Yoichi; Osaka, Futoshi
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 15
• Pages of publication: 1836 - 1841
• a: 8.6613 ± 0.0007 Å
• b: 10.9064 ± 0.0009 Å
• c: 13.7569 ± 0.0011 Å
• α: 81.397 ± 0.002°
• β: 72.028 ± 0.001°
• γ: 72.695 ± 0.002°
• Cell volume: 1177.77 ± 0.17 ų
• Cell temperature: 298 K
• Ambient diffraction temperature: 298 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0387
• Residual factor for significantly intense reflections: 0.0338
• Weighted residual factors for significantly intense reflections: 0.0905
• Weighted residual factors for all reflections included in the refinement: 0.0939
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No