Information card for entry 7006842

Structure parameters

• Common name: (Na(thf)6)(Na(thf)5)((Si(NCH2tBu)2C6H4)3)
• Formula: C92 H166 N6 Na2 O11 Si3
• Calculated formula: C92.04 H138 N6 Na2 O11 Si3
• Title of publication: Insights into the making of a stable silylene.
• Authors of publication: Gehrhus, Barbara; Hitchcock, Peter B.; Pongtavornpinyo, Ruti; Zhang, Lihong
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 15
• Pages of publication: 1847 - 1857
• a: 15.0722 ± 0.0001 Å
• b: 15.0722 ± 0.0001 Å
• c: 25.4341 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 5003.8 ± 0.08 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 176
• Hermann-Mauguin space group symbol: P 63/m
• Hall space group symbol: -P 6c
• Residual factor for all reflections: 0.076
• Residual factor for significantly intense reflections: 0.0671
• Weighted residual factors for significantly intense reflections: 0.1858
• Weighted residual factors for all reflections included in the refinement: 0.1932
• Goodness-of-fit parameter for all reflections included in the refinement: 1.085
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No