Information card for entry 7006958

Structure parameters

• Formula: C78 H58 B2 N6 Rh S6
• Calculated formula: C78 H58 B2 N6 Rh S6
• Title of publication: Thiacalix[3]pyridine produces a stable mononuclear rhodium(II) complex with mutual Jahn-Teller effect.
• Authors of publication: Hamazawa, Rika Tanaka; Nishioka, Takanori; Kinoshita, Isamu; Takui, Takeji; Santo, Ryoko; Ichimura, Akio
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 11
• Pages of publication: 1374 - 1376
• a: 11.3931 ± 0.0017 Å
• b: 13.966 ± 0.002 Å
• c: 20.879 ± 0.003 Å
• α: 101.008 ± 0.004°
• β: 94.527 ± 0.004°
• γ: 93.488 ± 0.003°
• Cell volume: 3241.1 ± 0.8 ų
• Cell temperature: 193.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0507
• Weighted residual factors for all reflections included in the refinement: 0.0681
• Goodness-of-fit parameter for all reflections included in the refinement: 1.076
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No