Information card for entry 7006996

Structure parameters

• Formula: C96 H132 Li4 N8 O4 Si2
• Calculated formula: C96 H132 Li4 N8 O4 Si2
• SMILES: [Li]123[N](c4c(C(C)C)cccc4C(C)C)=C(c4ccccc4)[N]1([Li]145)[Si](C)(C)[N]16C(c1ccccc1)=[N](c1c(cccc1C(C)C)C(C)C)[Li]61[N](c6c(cccc6C(C)C)C(C)C)=C(c6ccccc6)[N]41[Si](C)(C)[N]25C(c1ccccc1)=[N]3c1c(cccc1C(C)C)C(C)C.[Li]([O]1CCCC1)([O]1CCCC1)([O]1CCCC1)[O]1CCCC1
• Title of publication: A convenient route to silyl linked bis(amidinate) ligands and synthesis of group(I) metal derivatives.
• Authors of publication: Bai, Sheng-Di; Guo, Jian-Ping; Liu, Dian-Sheng
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 18
• Pages of publication: 2244 - 2250
• a: 20.4738 ± 0.0013 Å
• b: 11.3967 ± 0.0007 Å
• c: 21.0692 ± 0.0012 Å
• α: 90°
• β: 101.957 ± 0.002°
• γ: 90°
• Cell volume: 4809.5 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/n 1
• Hall space group symbol: -P 2yac
• Residual factor for all reflections: 0.1687
• Residual factor for significantly intense reflections: 0.0613
• Weighted residual factors for significantly intense reflections: 0.1497
• Weighted residual factors for all reflections included in the refinement: 0.1967
• Goodness-of-fit parameter for all reflections included in the refinement: 0.897
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No