Information card for entry 7007117

Structure parameters

• Common name: na
• Formula: C76.5 H125 Mn9 Mo5.17 N48 O34 Re0.83
• Calculated formula: C51 Mn6 Mo3.44 N32 O22.6667 Re0.56
• Title of publication: Symmetry-breaking substitutions of [Re(CN)8]3- into the centered, face-capped octahedral clusters (CH3OH)24M9M'6(CN)48 (M = Mn, Co; M = Mo, W).
• Authors of publication: Freedman, Danna E.; Bennett, Miriam V.; Long, Jeffrey R.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 23
• Pages of publication: 2829 - 2834
• a: 29.366 ± 0.003 Å
• b: 19.029 ± 0.002 Å
• c: 32.886 ± 0.004 Å
• α: 90°
• β: 114.532 ± 0.002°
• γ: 90°
• Cell volume: 16718 ± 3 ų
• Cell temperature: 178 K
• Ambient diffraction temperature: 178 ± 2 K
• Number of distinct elements: 7
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.1218
• Residual factor for significantly intense reflections: 0.0904
• Weighted residual factors for significantly intense reflections: 0.2166
• Weighted residual factors for all reflections included in the refinement: 0.227
• Goodness-of-fit parameter for all reflections included in the refinement: 1.579
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No