Information card for entry 7007166

Structure parameters

• Formula: C37.5 H57 Cl5 P2 Pd
• Calculated formula: C37.5 H56 Cl5.005 P2 Pd
• Title of publication: 1,8-Dimethylnaphthalene-bridged diphosphine ligands: synthesis and structural comparison of their palladium complexes.
• Authors of publication: Bellabarba, Ronan M.; Hammond, Colin; Forman, Grant S.; Tooze, Robert P.; Slawin, Alexandra M. Z.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 20
• Pages of publication: 2444 - 2449
• a: 12.898 ± 0.003 Å
• b: 17.223 ± 0.004 Å
• c: 18.723 ± 0.004 Å
• α: 83.18 ± 0.02°
• β: 76.28 ± 0.02°
• γ: 79.56 ± 0.02°
• Cell volume: 3961.1 ± 1.6 ų
• Cell temperature: 93 ± 2 K
• Ambient diffraction temperature: 93 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1806
• Residual factor for significantly intense reflections: 0.1059
• Weighted residual factors for significantly intense reflections: 0.2094
• Weighted residual factors for all reflections included in the refinement: 0.2592
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No