Catalytic applications of keto-stabilised phosphorus ylides based on a macrocyclic scaffold: calixarenes with one or two pendant Ni(P,O)-subunits as ethylene oligomerisation and polymerisation catalysts.
Authors of publication
Kuhn, Pierre; Sémeril, David; Jeunesse, Catherine; Matt, Dominique; Lutz, Pierre J.; Louis, Rémy; Neuburger, Markus
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2006
Journal issue
30
Pages of publication
3647 - 3659
a
10.127 ± 0.002 Å
b
16.167 ± 0.002 Å
c
20.818 ± 0.004 Å
α
86.82 ± 0.05°
β
83.22 ± 0.05°
γ
78.4 ± 0.05°
Cell volume
3313.7 ± 1.2 Å3
Cell temperature
173 ± 2 K
Ambient diffraction temperature
173 ± 2 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.2185
Residual factor for significantly intense reflections
0.0927
Weighted residual factors for significantly intense reflections
0.1949
Weighted residual factors for all reflections included in the refinement
0.2343
Goodness-of-fit parameter for all reflections included in the refinement
