Group 11 complexes with the bis(3,5-dimethylpyrazol-1-yl)methane ligand. How secondary bonds can influence the coordination environment of Ag(I): the role of coordinated water in [Ag2(mu-L)2(OH2)2](OTf)2.
Authors of publication
José Calhorda, Maria; Costa, Paulo J.; Crespo, Olga; Gimeno, M Concepción; Jones, Peter G.; Laguna, Antonio; Naranjo, Mar; Quintal, Susana; Shi, Yu-Jun; Villacampa, M. Dolores
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2006
Journal issue
34
Pages of publication
4104 - 4113
a
7.5202 ± 0.0008 Å
b
13.0771 ± 0.0014 Å
c
9.2673 ± 0.0011 Å
α
90°
β
95.981 ± 0.004°
γ
90°
Cell volume
906.41 ± 0.17 Å3
Cell temperature
153 ± 2 K
Ambient diffraction temperature
153 ± 2 K
Number of distinct elements
6
Space group number
11
Hermann-Mauguin space group symbol
P 1 21/m 1
Hall space group symbol
-P 2yb
Residual factor for all reflections
0.0522
Residual factor for significantly intense reflections
0.0368
Weighted residual factors for significantly intense reflections
0.0918
Weighted residual factors for all reflections included in the refinement
0.1006
Goodness-of-fit parameter for all reflections included in the refinement
