Information card for entry 7007484

Structure parameters

• Formula: C2 H6 Cs4.5 O46.75 Ru S Si W11
• Calculated formula: C2 H6 Cs4.5 O46.75 Ru S Si W11
• Title of publication: Structural characterization of mono-ruthenium substituted Keggin-type silicotungstates.
• Authors of publication: Sadakane, Masahiro; Tsukuma, Daisuke; Dickman, Michael H.; Bassil, Bassem; Kortz, Ulrich; Higashijima, Michio; Ueda, Wataru
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 35
• Pages of publication: 4271 - 4276
• a: 13.585 ± 0.0004 Å
• b: 20.2764 ± 0.0007 Å
• c: 18.1326 ± 0.0004 Å
• α: 90°
• β: 90.873 ± 0.001°
• γ: 90°
• Cell volume: 4994.1 ± 0.3 ų
• Cell temperature: 297 ± 2 K
• Ambient diffraction temperature: 297 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.088
• Residual factor for significantly intense reflections: 0.0518
• Weighted residual factors for significantly intense reflections: 0.1415
• Weighted residual factors for all reflections included in the refinement: 0.165
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No