Silver(I) complexation of linked 2,2'-dipyridylamine derivatives. Synthetic, solvent extraction, membrane transport and X-ray structural studies.
Authors of publication
Antonioli, Bianca; Bray, David J.; Clegg, Jack K.; Gloe, Kerstin; Gloe, Karsten; Kataeva, Olga; Lindoy, Leonard F.; McMurtrie, John C.; Steel, Peter J.; Sumby, Christopher J.; Wenzel, Marco
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2006
Journal issue
40
Pages of publication
4783 - 4794
a
9.132 ± 0.0015 Å
b
12.801 ± 0.002 Å
c
15.264 ± 0.003 Å
α
81.91 ± 0.003°
β
81.998 ± 0.003°
γ
71.44 ± 0.003°
Cell volume
1666.2 ± 0.5 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 ± 2 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0665
Residual factor for significantly intense reflections
0.0424
Weighted residual factors for significantly intense reflections
0.0846
Weighted residual factors for all reflections included in the refinement
0.0921
Goodness-of-fit parameter for all reflections included in the refinement
