Information card for entry 7007773

Structure parameters

• Formula: C74 H86 Co4 N8 O19
• Calculated formula: C73.839 H85.22 Co4 N8 O18.94
• Title of publication: Dinuclear Co(III)/Co(III) and Co(II)/Co(III) mixed-valent complexes: synthetic control of the cobalt oxidation level.
• Authors of publication: Fondo, Matilde; Ocampo, Noelia; García-Deibe, Ana M; Corbella, Montserrat; El Fallah, M. Salah; Cano, Joan; Sanmartín, Jesús; Bermejo, Manuel R.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 41
• Pages of publication: 4905 - 4913
• a: 10.469 ± 0.002 Å
• b: 11.682 ± 0.002 Å
• c: 28.92 ± 0.006 Å
• α: 90°
• β: 90.541 ± 0.004°
• γ: 90°
• Cell volume: 3536.7 ± 1.2 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1146
• Residual factor for significantly intense reflections: 0.0555
• Weighted residual factors for significantly intense reflections: 0.1184
• Weighted residual factors for all reflections included in the refinement: 0.1375
• Goodness-of-fit parameter for all reflections included in the refinement: 0.996
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No