Information card for entry 7007977

Structure parameters

• Formula: C42 H42 Cl2 N2 P2 Pd
• Calculated formula: C42 H42 Cl2 N2 P2 Pd
• Title of publication: Chiral bidentate aminophosphine ligands: synthesis, coordination chemistry and asymmetric catalysis.
• Authors of publication: Zijp, Eric J.; van der Vlugt, Jarl Ivar; Tooke, Duncan M.; Spek, Anthony L.; Vogt, Dieter
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2005
• Journal issue: 3
• Pages of publication: 512 - 517
• a: 11.333 ± 0.001 Å
• b: 26.0777 ± 0.001 Å
• c: 12.6339 ± 0.001 Å
• α: 90°
• β: 92.771 ± 0.001°
• γ: 90°
• Cell volume: 3729.4 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0279
• Residual factor for significantly intense reflections: 0.0219
• Weighted residual factors for significantly intense reflections: 0.0428
• Weighted residual factors for all reflections included in the refinement: 0.0444
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No