Information card for entry 7008095

Structure parameters

• Formula: C95 H134 Br3 O10 P2 Rh
• Calculated formula: C95 H98 Br3 O10 P2 Rh
• Title of publication: Rhodium hydride formation in the presence of a bulky monophosphite ligand: a spectroscopic and solid-state investigation.
• Authors of publication: Crous, Renier; Datt, Michael; Foster, Douglas; Bennie, Linette; Steenkamp, Casper; Huyser, Johan; Kirsten, Leo; Steyl, Gideon; Roodt, Andreas
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2005
• Journal issue: 6
• Pages of publication: 1108 - 1116
• a: 12.996 ± 0.005 Å
• b: 14.078 ± 0.005 Å
• c: 28.243 ± 0.005 Å
• α: 102.514 ± 0.005°
• β: 94.303 ± 0.005°
• γ: 104.057 ± 0.005°
• Cell volume: 4849 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1796
• Residual factor for significantly intense reflections: 0.0645
• Weighted residual factors for significantly intense reflections: 0.1155
• Weighted residual factors for all reflections included in the refinement: 0.1506
• Goodness-of-fit parameter for all reflections included in the refinement: 0.915
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No