Information card for entry 7008178

Structure parameters

• Common name: tetraphenylarsonium (N,N'-bis(2-Hydroxyiminopropionyl)buthane- 1,4-diamine) -nickelate(ii) trihydrate
• Chemical name: tetraphenylarsonium (N,N'-bis(2-Hydroxyiminopropionyl)buthane-1,4-diamine) -nickelate(II) trihydrate
• Formula: C34 H42 As N4 Ni O7.5
• Calculated formula: C34 H40.5 As N4 Ni O7.5
• Title of publication: Effect of metal ionic radius and chelate ring alternation motif on stabilization of trivalent nickel and copper in binuclear complexes with double cis-oximato bridges.
• Authors of publication: Kanderal, Olga M.; Kozlowski, Henryk; Dobosz, Agnieszka; Swiatek-Kozlowska, Jolanta; Meyer, Franc; Fritsky, Igor O.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2005
• Journal issue: 8
• Pages of publication: 1428 - 1437
• a: 22.274 ± 0.004 Å
• b: 20.539 ± 0.004 Å
• c: 15.231 ± 0.003 Å
• α: 90°
• β: 97.18 ± 0.03°
• γ: 90°
• Cell volume: 6913 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0616
• Residual factor for significantly intense reflections: 0.0419
• Weighted residual factors for significantly intense reflections: 0.0902
• Weighted residual factors for all reflections included in the refinement: 0.0982
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No