New bis-, tris- and tetrakis(pyrazolyl)borate ligands with 3-pyridyl and 4-pyridyl substituents: synthesis and coordination chemistry.
Authors of publication
Adams, Harry; Batten, Stuart R.; Davies, Graham M.; Duriska, Martin B.; Jeffery, John C.; Jensen, Paul; Lu, Jinzhen; Motson, Graham R.; Coles, Simon J.; Hursthouse, Michael B.; Ward, Michael D.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2005
Journal issue
11
Pages of publication
1910 - 1923
a
9.2506 ± 0.0013 Å
b
12.3819 ± 0.0017 Å
c
19.887 ± 0.003 Å
α
90°
β
94.968 ± 0.002°
γ
90°
Cell volume
2269.3 ± 0.6 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 ± 2 K
Number of distinct elements
5
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.0322
Residual factor for significantly intense reflections
0.0263
Weighted residual factors for significantly intense reflections
0.0631
Weighted residual factors for all reflections included in the refinement
0.0659
Goodness-of-fit parameter for all reflections included in the refinement
