New bis-, tris- and tetrakis(pyrazolyl)borate ligands with 3-pyridyl and 4-pyridyl substituents: synthesis and coordination chemistry.
Authors of publication
Adams, Harry; Batten, Stuart R.; Davies, Graham M.; Duriska, Martin B.; Jeffery, John C.; Jensen, Paul; Lu, Jinzhen; Motson, Graham R.; Coles, Simon J.; Hursthouse, Michael B.; Ward, Michael D.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2005
Journal issue
11
Pages of publication
1910 - 1923
a
9.5334 ± 0.0013 Å
b
13.7358 ± 0.0018 Å
c
13.8959 ± 0.0019 Å
α
70.983 ± 0.002°
β
84.41 ± 0.002°
γ
70.248 ± 0.002°
Cell volume
1619 ± 0.4 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 ± 2 K
Number of distinct elements
6
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0864
Residual factor for significantly intense reflections
0.0524
Weighted residual factors for significantly intense reflections
0.1198
Weighted residual factors for all reflections included in the refinement
0.1326
Goodness-of-fit parameter for all reflections included in the refinement
