Information card for entry 7008509

Structure parameters

• Formula: C16 H20 O2 P2 Pb Se4
• Calculated formula: C16 H19 O2 P2 Pb Se4
• Title of publication: Synthesis and structure of novel [Ph(RO)PSe2]- complexes.
• Authors of publication: Gray, Ian P.; Slawin, Alexandra M. Z.; Woollins, J. Derek
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2005
• Journal issue: 12
• Pages of publication: 2188 - 2194
• a: 6.4975 ± 0.0007 Å
• b: 13.1066 ± 0.0013 Å
• c: 14.502 ± 0.002 Å
• α: 110.741 ± 0.014°
• β: 97.96 ± 0.02°
• γ: 100.16 ± 0.02°
• Cell volume: 1109.4 ± 0.3 ų
• Cell temperature: 93 ± 2 K
• Ambient diffraction temperature: 93 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0469
• Residual factor for significantly intense reflections: 0.04
• Weighted residual factors for significantly intense reflections: 0.0957
• Weighted residual factors for all reflections included in the refinement: 0.1025
• Goodness-of-fit parameter for all reflections included in the refinement: 0.602
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No