Information card for entry 7008516

Structure parameters

• Formula: C37 H18 Cl4 O36 Os10 Rh6
• Calculated formula: C37 H18 Cl4 O36 Os10 Rh6
• SMILES: [Os]1234([Os]56([Rh]789%10%111([Os]1%12([Os]7([Rh]7%1391([Os]19([Rh]258([Cl]71)(C#[O])[H]9)(C#[O])(C#[O])(C#[O])[H]%13)C#[O])(C#[O])(C#[O])(C#[O])([H]%12)[H]%10)(C#[O])(C#[O])(C#[O])[H]%11)(C#[O])([H]4)[H]6)(C#[O])(C#[O])(C#[O])[H]3)(C#[O])(C#[O])C#[O].ClCCl
• Title of publication: Synthesis and structural characterization of a series of high-hydride content osmium-rhodium carbonyl complexes by the hydrogenation of arene-coordinated clusters.
• Authors of publication: Lau, Jasmine Po-Kwan; Wong, Wing-Tak
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2005
• Journal issue: 15
• Pages of publication: 2579 - 2587
• a: 8.522 ± 0.002 Å
• b: 21.992 ± 0.005 Å
• c: 37.291 ± 0.01 Å
• α: 90°
• β: 91.15 ± 0.01°
• γ: 90°
• Cell volume: 6988 ± 3 ų
• Cell temperature: 298.1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.058
• Weighted residual factors for all reflections included in the refinement: 0.063
• Goodness-of-fit parameter for all reflections included in the refinement: 1.125
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No