Information card for entry 7008530

Structure parameters

• Formula: C46 H37 B N3 O1.73 Rh S3
• Calculated formula: C46 H37 B N3 O1.73 Rh S3
• Title of publication: Selective oxygenation of amphiphilic thiacalix[3]pyridine Rh(I) diene complexes in both water and organic solvents.
• Authors of publication: Nishioka, Takanori; Onishi, Yusuke; Nakajo, Kunio; Guo-Xin, Jin; Tanaka, Rika; Kinoshita, Isamu
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2005
• Journal issue: 12
• Pages of publication: 2130 - 2137
• a: 10.17 ± 0.002 Å
• b: 11.684 ± 0.003 Å
• c: 17.496 ± 0.004 Å
• α: 104.214 ± 0.004°
• β: 104.41 ± 0.004°
• γ: 94.148 ± 0.003°
• Cell volume: 1932.1 ± 0.8 ų
• Cell temperature: 193.2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0494
• Weighted residual factors for all reflections included in the refinement: 0.076
• Goodness-of-fit parameter for all reflections included in the refinement: 0.999
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No