Information card for entry 7008579

Structure parameters

• Formula: C88 H90 F24 N18 O10 P4 Ru2
• Calculated formula: C88 H87 F24 N18 O10 P4 Ru2
• Title of publication: Formation of [2 + 2] diruthenium(II) metallomacrocycles from ligands containing 2,2':6',2''-terpyridine domains linked through flexible polyethyleneoxy spacers.
• Authors of publication: Constable, Edwin C.; Housecroft, Catherine E.; Neuburger, Markus; Schaffner, Silvia; Smith, Christopher B.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2005
• Journal issue: 13
• Pages of publication: 2259 - 2267
• a: 13.746 ± 0.0014 Å
• b: 14.81 ± 0.004 Å
• c: 15.067 ± 0.003 Å
• α: 100.87 ± 0.02°
• β: 111.407 ± 0.009°
• γ: 111.286 ± 0.018°
• Cell volume: 2471.9 ± 1.1 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1073
• Residual factor for significantly intense reflections: 0.0598
• Weighted residual factors for all reflections: 0.0712
• Weighted residual factors for significantly intense reflections: 0.0535
• Weighted residual factors for all reflections included in the refinement: 0.0535
• Goodness-of-fit parameter for all reflections included in the refinement: 1.1083
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No