Information card for entry 7008582

Structure parameters

• Common name: Lithium bis(phenylsulfonyl)imide pyridine solvate
• Formula: C22 H20 Li N3 O4 S2
• Calculated formula: C22 H20 Li N3 O4 S2
• Title of publication: Synthesis of mono- and geminal dimetalated carbanions of bis(phenylsulfonyl)methane using alkali metal bases and structural comparisons with lithiated bis(phenylsulfonyl)imides.
• Authors of publication: MacDougall, Dugald J.; Kennedy, Alan R.; Noll, Bruce C.; Henderson, Kenneth W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2005
• Journal issue: 12
• Pages of publication: 2084 - 2091
• a: 10.7604 ± 0.0006 Å
• b: 12.8589 ± 0.0007 Å
• c: 16.3444 ± 0.0009 Å
• α: 90°
• β: 105.549 ± 0.001°
• γ: 90°
• Cell volume: 2178.8 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0376
• Residual factor for significantly intense reflections: 0.0352
• Weighted residual factors for significantly intense reflections: 0.0954
• Weighted residual factors for all reflections included in the refinement: 0.0975
• Goodness-of-fit parameter for all reflections included in the refinement: 1.051
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No