Information card for entry 7008584

Structure parameters

• Formula: C17 H19 Li O5 S2
• Calculated formula: C17 H19 Li O5 S2
• Title of publication: Synthesis of mono- and geminal dimetalated carbanions of bis(phenylsulfonyl)methane using alkali metal bases and structural comparisons with lithiated bis(phenylsulfonyl)imides.
• Authors of publication: MacDougall, Dugald J.; Kennedy, Alan R.; Noll, Bruce C.; Henderson, Kenneth W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2005
• Journal issue: 12
• Pages of publication: 2084 - 2091
• a: 5.7976 ± 0.0004 Å
• b: 34.489 ± 0.003 Å
• c: 9.0798 ± 0.0008 Å
• α: 90°
• β: 103.882 ± 0.002°
• γ: 90°
• Cell volume: 1762.5 ± 0.3 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1131
• Residual factor for significantly intense reflections: 0.0559
• Weighted residual factors for significantly intense reflections: 0.1149
• Weighted residual factors for all reflections included in the refinement: 0.1339
• Goodness-of-fit parameter for all reflections included in the refinement: 1.011
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No