Information card for entry 7008589

Structure parameters

• Chemical name: tetra(15-crown-5)heptakis(mu-fluoro)tetrakisgadolinium(III) pentakis(hexafluoroarsenate) sulphur dioxide solvate
• Formula: C40 H80 As5 F37 Gd4 O32 S6
• Calculated formula: C40 H80 As5 F37 Gd4 O32 S6
• Title of publication: Stabilising small clusters: synthesis and characterisation of thermolabile [Gd4F7(15-crown-5)4][AsF6]5.6 SO2.
• Authors of publication: Deacon, Glen B.; Evans, David J.; Junk, Peter C.; Lork, Enno; Mews, Rüdiger; Zemva, Boris
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2005
• Journal issue: 13
• Pages of publication: 2237 - 2238
• a: 13.712 ± 0.003 Å
• b: 13.783 ± 0.003 Å
• c: 24.527 ± 0.005 Å
• α: 86.32 ± 0.03°
• β: 84.45 ± 0.03°
• γ: 73.91 ± 0.03°
• Cell volume: 4429.6 ± 1.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1261
• Residual factor for significantly intense reflections: 0.0768
• Weighted residual factors for significantly intense reflections: 0.176
• Weighted residual factors for all reflections included in the refinement: 0.2033
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No