Information card for entry 7008635

Structure parameters

• Formula: C44.72 H43.44 N2 O9.18 Sb2
• Calculated formula: C44.72 H43.44 N2 O9.18 Sb2
• Title of publication: Multidentate aryloxide and oxo-aryloxide complexes of antimony: synthesis and structural characterization of [eta4-N(o-C6H4O)3]Sb(OSMe2), {{[eta3-N(o-C6H4OH)- (o-C6H4O)2]Sb}2(mu2-O)}2 and {[eta3-PhN(o-C6H4O)2]Sb}4(mu3-O)2.
• Authors of publication: Tanski, Joseph M.; Kelly, Bryte V.; Parkin, Gerard
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2005
• Journal issue: 14
• Pages of publication: 2442 - 2447
• a: 13.1256 ± 0.0007 Å
• b: 13.3738 ± 0.0008 Å
• c: 14.4188 ± 0.0008 Å
• α: 111.544 ± 0.001°
• β: 99.969 ± 0.001°
• γ: 108.335 ± 0.001°
• Cell volume: 2111.9 ± 0.2 ų
• Cell temperature: 243 ± 2 K
• Ambient diffraction temperature: 243 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0471
• Residual factor for significantly intense reflections: 0.0335
• Weighted residual factors for significantly intense reflections: 0.088
• Weighted residual factors for all reflections included in the refinement: 0.0962
• Goodness-of-fit parameter for all reflections included in the refinement: 1.007
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No