Information card for entry 7008701

Structure parameters

• Formula: C33 H33 F12 Gd N2 O11 V
• Calculated formula: C33 H33 F12 Gd N2 O11 V
• Title of publication: The first example of a hetero-tetranuclear [(VO)Gd](2) complex: synthesis, crystal structure and magnetic properties of [VOLGd(hfa)(2)CH(3)OH](2).2CH(3)OH.2(CH(3))(2)CO.
• Authors of publication: Costes, Jean-Pierre; Shova, Sergiu; Juan, Juan Modesto Clemente; Suet, Nicolas
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2005
• Journal issue: 17
• Pages of publication: 2830 - 2832
• a: 28.631 ± 0.006 Å
• b: 16.612 ± 0.003 Å
• c: 17.346 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8250 ± 3 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 7
• Space group number: 56
• Hermann-Mauguin space group symbol: P c c n
• Hall space group symbol: -P 2ab 2ac
• Residual factor for all reflections: 0.0624
• Residual factor for significantly intense reflections: 0.0336
• Weighted residual factors for significantly intense reflections: 0.0587
• Weighted residual factors for all reflections included in the refinement: 0.0664
• Goodness-of-fit parameter for all reflections included in the refinement: 0.977
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No