Information card for entry 7008709

Structure parameters

• Formula: C14.5 H24.5 Cl1.5 Li0.5 N O Si Th0.5
• Calculated formula: C14.5 H24.5 Cl1.5 Li0.5 N O Si Th0.5
• Title of publication: Synthesis and structure of diamido ether uranium(IV) and thorium(IV) halide "ate" complexes and their conversion to salt-free bis(alkyl) complexes.
• Authors of publication: Jantunen, Kimberly C.; Haftbaradaran, Farzad; Katz, Michael J.; Batchelor, Raymond J.; Schatte, Gabriele; Leznoff, Daniel B.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2005
• Journal issue: 18
• Pages of publication: 3083 - 3091
• a: 24.157 ± 0.005 Å
• b: 17.397 ± 0.004 Å
• c: 9.239 ± 0.002 Å
• α: 90°
• β: 99.17 ± 0.02°
• γ: 90°
• Cell volume: 3833.2 ± 1.5 ų
• Cell temperature: 293 K
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 8
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.0761
• Residual factor for significantly intense reflections: 0.0469
• Weighted residual factors for all reflections: 0.0873
• Weighted residual factors for significantly intense reflections: 0.0597
• Weighted residual factors for all reflections included in the refinement: 0.0597
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0002
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No