Information card for entry 7009126

Structure parameters

• Formula: C29 H30 P2 Pd S2
• Calculated formula: C29 H26 P2 Pd S2
• Title of publication: A new access to palladium‒phosphine chemistry. Formation of polynuclear palladium compounds via the oxidation of ligands in simple palladium(II) complexes
• Authors of publication: Su, Weiping; Cao, Rong; Hong, Maochun; Wu, Daxu; Lu, Jiaxi
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 9
• Pages of publication: 1527
• a: 10.354 ± 0.002 Å
• b: 25.041 ± 0.005 Å
• c: 11.332 ± 0.002 Å
• α: 90°
• β: 107.87 ± 0.03°
• γ: 90°
• Cell volume: 2796.4 ± 1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0488
• Residual factor for significantly intense reflections: 0.0357
• Weighted residual factors for all reflections: 0.1024
• Weighted residual factors for significantly intense reflections: 0.1006
• Goodness-of-fit parameter for all reflections: 1.056
• Goodness-of-fit parameter for significantly intense reflections: 1.143
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No