Information card for entry 7009146

Structure parameters

• Formula: C60 H80 Cl2 N O4 P Pd
• Calculated formula: C60 H80 Cl2 N O4 P Pd
• Title of publication: Calix[4]arene derived phosphites: their hydrolytic stability and complexes with gold(I), platinum(II,0), palladium(II) and iridium(I)
• Authors of publication: Cobley, Christopher J.; Ellis, Dianne D.; Orpen, A. Guy; Pringle, Paul G.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 7
• Pages of publication: 1101
• a: 22.871 ± 0.004 Å
• b: 13.852 ± 0.003 Å
• c: 18.117 ± 0.003 Å
• α: 90°
• β: 93.104 ± 0.012°
• γ: 90°
• Cell volume: 5731.2 ± 1.9 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 7
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0459
• Residual factor for significantly intense reflections: 0.0447
• Weighted residual factors for all reflections: 0.1182
• Weighted residual factors for significantly intense reflections: 0.1163
• Goodness-of-fit parameter for all reflections: 1.029
• Goodness-of-fit parameter for significantly intense reflections: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No