Crystallography Open Database

Information card for entry 7009320

Preview

Coordinates	7009320.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C37 H29 N2 O8 Os3 P
Calculated formula	C37 H29 N2 O8 Os3 P
Title of publication	Complexation and metallation of the multifunctional [Ph2P(o-C6H4)CHN(CH2)2(o-C5H4N)] ligand on triosmium carbonyl clusters
Authors of publication	Yeh, Wen-Yann; Yang, Ching-Chao; Peng, Shie-Ming; Lee, Gene-Hsiang
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2000
Journal issue	10
Pages of publication	1649
a	9.572 ± 0.0001 Å
b	10.6385 ± 0.0002 Å
c	20.2534 ± 0.0002 Å
α	79.228 ± 0.001°
β	88.699 ± 0.001°
γ	68.027 ± 0.001°
Cell volume	1876.39 ± 0.05 Å³
Cell temperature	295 ± 2 K
Ambient diffraction temperature	295 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0453
Residual factor for significantly intense reflections	0.031
Weighted residual factors for all reflections	0.0839
Weighted residual factors for significantly intense reflections	0.0729
Goodness-of-fit parameter for all reflections	1.134
Goodness-of-fit parameter for significantly intense reflections	1.094
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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