Information card for entry 7010002

Structure parameters

• Formula: C9.87 H9.87 Cl4 N1.97 Pb
• Calculated formula: C9.866 H9.866 Cl4 N1.9732 Pb1.0134
• Title of publication: Organic‒inorganic hybrid solids: control of perhalometallate solid state structures †
• Authors of publication: Gillon, Amy L.; Lewis, Gareth R.; Orpen, A. Guy; Rotter, Sarah; Starbuck, Jonathan; Wang, Xi-Meng; Rodríguez-Martín, Yolanda; Ruiz-Pérez, Catalina
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 21
• Pages of publication: 3897
• a: 13.012 ± 0.003 Å
• b: 16.458 ± 0.003 Å
• c: 7.392 ± 0.0011 Å
• α: 90°
• β: 119.997 ± 0.012°
• γ: 90°
• Cell volume: 1371 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0313
• Residual factor for significantly intense reflections: 0.028
• Weighted residual factors for significantly intense reflections: 0.0639
• Weighted residual factors for all reflections included in the refinement: 0.0647
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No