Information card for entry 7010129

Structure parameters

• Formula: C77.5 H71 Cl11 Co2 N4 P4
• Calculated formula: C77.5 H71 Cl11 Co2 N4 P4
• Title of publication: Sterically hindered iminophosphorane complexes of vanadium, iron, cobalt and nickel: a synthetic, structural and catalytic study †
• Authors of publication: Al-Benna, Sarah; Sarsfield, Mark J.; Thornton-Pett, Mark; Ormsby, Daniel L.; Maddox, Peter J.; Brès, Philippe; Bochmann, Manfred
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 23
• Pages of publication: 4247
• a: 14.555 ± 0.0008 Å
• b: 15.5053 ± 0.0007 Å
• c: 18.2403 ± 0.0009 Å
• α: 89.686 ± 0.003°
• β: 68.223 ± 0.002°
• γ: 85.079 ± 0.003°
• Cell volume: 3807.1 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1416
• Residual factor for significantly intense reflections: 0.0974
• Weighted residual factors for significantly intense reflections: 0.2222
• Weighted residual factors for all reflections included in the refinement: 0.2434
• Goodness-of-fit parameter for all reflections included in the refinement: 1.11
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No