Information card for entry 7010247
| Formula |
C47 H57 F6 N3 P Rh |
| Calculated formula |
C47 H57 F6 N3 P Rh |
| Title of publication |
An investigation of 1,4,7-tri(4-alkynyl)-1,4,7-triazacyclononanes: ligand synthesis and metal co-ordination chemistry † |
| Authors of publication |
Baker, Murray V.; Brown, David H.; Skelton, Brian W.; White, Allan H. |
| Journal of publication |
Journal of the Chemical Society, Dalton Transactions |
| Year of publication |
2000 |
| Journal issue |
24 |
| Pages of publication |
4607 |
| a |
11.485 ± 0.001 Å |
| b |
12.312 ± 0.002 Å |
| c |
30.35 ± 0.004 Å |
| α |
90° |
| β |
90° |
| γ |
90° |
| Cell volume |
4291.6 ± 1 Å3 |
| Cell temperature |
153 K |
| Ambient diffraction temperature |
153 K |
| Number of distinct elements |
6 |
| Space group number |
19 |
| Hermann-Mauguin space group symbol |
P 21 21 21 |
| Hall space group symbol |
P 2ac 2ab |
| Residual factor for all reflections |
0.05 |
| Residual factor for significantly intense reflections |
0.038 |
| Weighted residual factors for all reflections |
0.044 |
| Weighted residual factors for all reflections included in the refinement |
0.041 |
| Goodness-of-fit parameter for all reflections |
1.418 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.417 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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https://www.crystallography.net/7010247.html
