Information card for entry 7010609

Structure parameters

• Formula: C32 H72 Ga2 K2 N8
• Calculated formula: C32 H72 Ga2 K2 N8
• Title of publication: In further pursuit of the carbene analogy: preparation and crystal structure of (N,N,N ',N '-tetramethylethylenediamine)potassium [cis-ethene-1,2-di(tert-butylamido)]gallate(I)
• Authors of publication: Schmidt, Eva Susanne; Schier, Annette; Schmidbaur, Hubert
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 5
• Pages of publication: 505
• a: 10.3925 ± 0.0002 Å
• b: 10.7648 ± 0.0002 Å
• c: 10.9534 ± 0.0003 Å
• α: 101.728 ± 0.001°
• β: 92.051 ± 0.001°
• γ: 114.45 ± 0.001°
• Cell volume: 1082.28 ± 0.04 ų
• Cell temperature: 143 ± 2 K
• Ambient diffraction temperature: 143 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0333
• Residual factor for significantly intense reflections: 0.0309
• Weighted residual factors for significantly intense reflections: 0.074
• Weighted residual factors for all reflections included in the refinement: 0.0753
• Goodness-of-fit parameter for all reflections included in the refinement: 1.067
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No