Information card for entry 7010744

Structure parameters

• Common name: (NacNacLi)2
• Formula: C29 H39.5 Li N2
• Calculated formula: C29 H39.5 Li N2
• Title of publication: The synthesis and structure of lithium derivatives of the sterically encumbered β-diketiminate ligand [{(2,6-Pri2H3C6)N(CH3)C}2CH]‒, and a modified synthesis of the aminoimine precursor
• Authors of publication: Stender, Matthias; Wright, Robert J.; Eichler, Barrett E.; Prust, Jörg; Olmstead, Marilyn M.; Roesky, Herbert W.; Power, Philip P.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 23
• Pages of publication: 3465
• a: 12.4708 ± 0.0014 Å
• b: 14.0455 ± 0.0016 Å
• c: 15.1235 ± 0.0017 Å
• α: 90.765 ± 0.003°
• β: 91.189 ± 0.003°
• γ: 102.979 ± 0.003°
• Cell volume: 2580.3 ± 0.5 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1546
• Residual factor for significantly intense reflections: 0.0769
• Weighted residual factors for significantly intense reflections: 0.1956
• Weighted residual factors for all reflections included in the refinement: 0.2406
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No