Information card for entry 7010806

Structure parameters

• Formula: C24 Al2 F55 I6 O6 P3
• Calculated formula: C24 Al2 F55 I6 O6 P3
• Title of publication: Reactions of P4 and I2 with Ag[Al(OC(CF3)3)4]: from elusive polyphosphorus cations to subvalent P3I6+ and phosphorus rich P5I2+
• Authors of publication: Ingo Krossing
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2002
• Journal issue: 4
• Pages of publication: 500 - 512
• a: 10.375 ± 0.002 Å
• b: 10.757 ± 0.002 Å
• c: 26.591 ± 0.005 Å
• α: 95.07 ± 0.03°
• β: 92.84 ± 0.03°
• γ: 98.48 ± 0.03°
• Cell volume: 2917.8 ± 1 ų
• Cell temperature: 175 K
• Ambient diffraction temperature: 175 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.2357
• Residual factor for significantly intense reflections: 0.0744
• Weighted residual factors for significantly intense reflections: 0.1636
• Weighted residual factors for all reflections included in the refinement: 0.1976
• Goodness-of-fit parameter for all reflections included in the refinement: 0.676
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No