Information card for entry 7010855

Structure parameters

• Formula: C27.5 H30 Cl3 N O4 P Rh
• Calculated formula: C27.5 H29 Cl3 N O4 P Rh
• Title of publication: Synthesis and structure of novel rhodium complexes of multi-functionalised amine-phosphine ligands
• Authors of publication: Clarke, Matthew L.; Slawin, Alexandra M. Z.; Wheatley, Matthew V.; Woollins, J. Derek
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 23
• Pages of publication: 3421
• a: 32.668 ± 0.002 Å
• b: 8.1102 ± 0.0005 Å
• c: 24.401 ± 0.002 Å
• α: 90°
• β: 102.928 ± 0.002°
• γ: 90°
• Cell volume: 6301 ± 0.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1026
• Residual factor for significantly intense reflections: 0.0574
• Weighted residual factors for all reflections: 0.2421
• Weighted residual factors for significantly intense reflections: 0.146
• Goodness-of-fit parameter for all reflections: 0.868
• Goodness-of-fit parameter for significantly intense reflections: 0.898
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No