Information card for entry 7010862

Structure parameters

• Formula: C38 H64 O2 P2 Rb2
• Calculated formula: C38 H64 O2 P2 Rb2
• Title of publication: Syntheses and solid-state structures of [{K(THF)2(PHTipp)K(THF)(μ-THF)(PHTipp)}x]2 and [Rb(THF)(PHTipp)]x (Tipp = 2,4,6-Pri3C6H2)
• Authors of publication: Christoph Frenzel; Fernando Somoza Jr.; Steffen Blaurock; Evamarie Hey-Hawkins
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2001
• Journal issue: 20
• Pages of publication: 3115 - 3118
• a: 13.165 ± 0.003 Å
• b: 13.643 ± 0.003 Å
• c: 13.807 ± 0.003 Å
• α: 113.61 ± 0.03°
• β: 103.67 ± 0.03°
• γ: 91.66 ± 0.03°
• Cell volume: 2186.5 ± 1.1 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1259
• Residual factor for significantly intense reflections: 0.0529
• Weighted residual factors for significantly intense reflections: 0.1389
• Weighted residual factors for all reflections included in the refinement: 0.1865
• Goodness-of-fit parameter for all reflections included in the refinement: 0.932
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No